The graphene was synthesized by two routes the 1st one application of conventional sonication in case of Tri-chloro-acetic 75% H2SO3 for 60hrs while 2nd is combined sonication (60 hrs) plus laser irradiations for 30hrs. The yields of two routes are collected and compared structurally to check and investigate the effect of laser on structure quality and amount of yield obtained. Results indicated that combined route gave yield higher than conventional route by ratio ~ 39%. AFM-investigations were performed to characterize nano-structural features of produced graphene. Furthermore raman spectra were measured to confirm graphene formation.
Published in | Radiation Science and Technology (Volume 2, Issue 2) |
DOI | 10.11648/j.rst.20160202.13 |
Page(s) | 25-29 |
Creative Commons |
This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited. |
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Copyright © The Author(s), 2017. Published by Science Publishing Group |
Nd-Laser, Synthesis, Dispersion, AFM, Graphene, Raman Spectra
[1] | Soldano, C., Mahmood, A. & Dujardin, E. (2010). Production, Properties and Potential of Graphene. Carbon, 48: 2127-2150. |
[2] | Geim, A. K. & Novoselov, K. S. (2007). The Rise of Grapehene. Nature Materials, 6: 183-191. |
[3] | Park, S. & Ruoff, R. D. (2009). Chemical methods for the production of graphenes. Nature Nanotechnology 4: 217-224. |
[4] | Novoselov, K. S., Geim, A. K., Morozov, S. V., Jiang, D., Zhang, Y., Dubonos S. V., Grigorieva, I. V. & Firsov, A. A., (2004). Electric Field Effect in Atomically Thin Carbon Films. Science, 306: 666-669. |
[5] | Hummers, W. S. & Offeman, R. E. (1958). Preparation of Graphite Oxide. Journal of the American Chemical Society, 80 (6): 1339. |
[6] | Dressehaus, M. S. & Dressehaus, D. (2009). Intercalation Compounds of Graphite. Advance Physics, 51 (1): 1-186. |
[7] | Schniepp, H. C., Li, J. L., McAllister, M. J., Sai, H., Herrera-Alonso, M. & Adamson D. H. (2006). Functionalized Single Graphene Sheets Derived from Splitting Graphite Oxide. Journal of Physical Chemistry B, 110 (17): 8535-8539. |
[8] | McAllister, M. J., Li, J. L., Adamson, D. H., Schniepp, H. C., Abdala, A. A. & Liu, J. (2007). Single Sheet Functionalized Graphene by Oxidation and Thermal Expansion of Graphite. Chemistry of Material, 19 (18): 4396-4404. |
[9] | Li, D., Muller, M. B. Gilje, S., Kaner, R. B. & Wallace, G. G. (2008). Processable Aqueous Dispersions of Graphene Nanosheets. Nature Nanotechnology, 3 (2): 101-105. |
[10] | Chen, Y., Qi, Y., Tai, Z., Yan, X., Zhu, F., & Xue, Q. (2012). Preparation, mechanical properties and biocompatibility of graphene oxide/ultrahigh molecular weight polyethylene composites. European Polymer Journal, 48: 1026-1033. |
[11] | Zhou, X. Z., Huang, X., Qi, X. Y., Wu, S. X., Xue, C., Boey F. Y. C., Yan, Q., Chen, P. & Zhang, H. (2009) In situ synthesis of metal nanoparticles on single-layer graphene oxide and reduced graphene oxide surfaces. Journal of Physical Chemistry C, 113: 10842–10846. |
[12] | Stankovich, S., Dikin, D. A., Compton, O. C., Dommett, G. H. B., Ruoff, R. S. & Nguyen S. T. (2010). Systematic Post-assembly Modification of Graphene Oxide Paper with Primary Alkylamines. Chemistry of Material, 22: 4153-4157. |
[13] | Hernandez, Y., Nicolosi, V., Lotya, M., Blighe, F. M., Sun, Z. & De, S. (2008). High-yield Production of Graphene by Liquid-phase Exfoliation of Graphite. Nature Nanotechnology, 3 (9): 563-568. |
[14] | Alhuthali A., El-Nahass M. M., Atta A. A., Abd El-Raheem M. M., Elsabawy K. M., Hassanien A. M. (2015). Study of topological morphology and optical properties of SnO2 thin films deposited by RF sputtering technique, Journal of Luminescence, 158: 165-171. |
[15] | Elsabawy K. M. (2015) Hyperfine Nano-Structural investigations of Solid PhaseCefixime Antibiotic Drug, Inter. Journal of Chemical Concepts, 1, 1: 38-43. |
[16] | Elsabawy K. M. (2016) Nano-Investigations on Surface Topology and Structural Suitability of Gramicidine Drug J. of World Scientific News, WSN 30: 57-67. |
[17] | Elsabawy K. M. (2011), Synthesis of Tunable MgB2/Nano-Graphene/MgB2 –Josephson Junction Like Structure for Electronic Devices, (2011), RSC-Advances Journal, Royal Society of Chemistry, 1: 964-967. |
[18] | Changjing F., Guogang Z., Haijun Z., Shuang L. (2013), Evaluation and Characterization of Reduced Graphene Oxide Nanosheets as Anode Materials for Lithium-Ion Batteries, Int. J. Electrochem. Sci., 8: 6269–6280. |
[19] | Geim, A. K. & Novoselov, K. S. (2007). The Rise of Grapehene. Nature Materials, 6: 183-191. |
[20] | Park, S. & Ruoff, R. D. (2009). Chemical methods for the production of graphenes. Nature Nanotechnology 4: 217-224. |
APA Style
Khaled M. Elsabawy. (2017). 2D-Growth Rate Promotion of Graphene via Intensive Nd-Laser/Sonication Irradiations. Radiation Science and Technology, 2(2), 25-29. https://doi.org/10.11648/j.rst.20160202.13
ACS Style
Khaled M. Elsabawy. 2D-Growth Rate Promotion of Graphene via Intensive Nd-Laser/Sonication Irradiations. Radiat. Sci. Technol. 2017, 2(2), 25-29. doi: 10.11648/j.rst.20160202.13
@article{10.11648/j.rst.20160202.13, author = {Khaled M. Elsabawy}, title = {2D-Growth Rate Promotion of Graphene via Intensive Nd-Laser/Sonication Irradiations}, journal = {Radiation Science and Technology}, volume = {2}, number = {2}, pages = {25-29}, doi = {10.11648/j.rst.20160202.13}, url = {https://doi.org/10.11648/j.rst.20160202.13}, eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.rst.20160202.13}, abstract = {The graphene was synthesized by two routes the 1st one application of conventional sonication in case of Tri-chloro-acetic 75% H2SO3 for 60hrs while 2nd is combined sonication (60 hrs) plus laser irradiations for 30hrs. The yields of two routes are collected and compared structurally to check and investigate the effect of laser on structure quality and amount of yield obtained. Results indicated that combined route gave yield higher than conventional route by ratio ~ 39%. AFM-investigations were performed to characterize nano-structural features of produced graphene. Furthermore raman spectra were measured to confirm graphene formation.}, year = {2017} }
TY - JOUR T1 - 2D-Growth Rate Promotion of Graphene via Intensive Nd-Laser/Sonication Irradiations AU - Khaled M. Elsabawy Y1 - 2017/01/07 PY - 2017 N1 - https://doi.org/10.11648/j.rst.20160202.13 DO - 10.11648/j.rst.20160202.13 T2 - Radiation Science and Technology JF - Radiation Science and Technology JO - Radiation Science and Technology SP - 25 EP - 29 PB - Science Publishing Group SN - 2575-5943 UR - https://doi.org/10.11648/j.rst.20160202.13 AB - The graphene was synthesized by two routes the 1st one application of conventional sonication in case of Tri-chloro-acetic 75% H2SO3 for 60hrs while 2nd is combined sonication (60 hrs) plus laser irradiations for 30hrs. The yields of two routes are collected and compared structurally to check and investigate the effect of laser on structure quality and amount of yield obtained. Results indicated that combined route gave yield higher than conventional route by ratio ~ 39%. AFM-investigations were performed to characterize nano-structural features of produced graphene. Furthermore raman spectra were measured to confirm graphene formation. VL - 2 IS - 2 ER -