A Review: Sample Preparation Methods for the Pesticide Residue Analysis in Food Samples

Shibiru Eticha

doi:doi:10.11648/j.ijpc.20200606.11

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A Review: Sample Preparation Methods for the Pesticide Residue Analysis in Food Samples

Shibiru Eticha

Published in International Journal of Pharmacy and Chemistry (Volume 6, Issue 6)

Received: 16 September 2020 Accepted: 30 September 2020 Published: 11 November 2020

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Abstract

The pesticide residues in foods have received increasing attention as one of the most important food safety issues. Therefore, more strict regulations on the maximum residue limits (MRLs) for pesticides in foods have been established in many countries and health organizations, based on the sensitive and reliable analysis methods of pesticide residues. However, the analysis of pesticide residues is a continuing challenge mainly because of the small quantities of analytes as well as the large amounts of interfering substances which can be co-extracted with them, often leading to experimental errors and damage to the Analytical instruments. Thus, extensive sample preparation is often required for the pesticide residue analysis for the effective extraction of the analytes and removal of the interferences. This paper focuses on reviewing the recent development in the sample preparation methods for the pesticide residue analysis in some food samples. The methods include: Liquid-Liquid extraction (LLE), Solid-Phase extraction (SPE), Matrix Solid-Phase Dispersion (MSPD), Solid-Phase Micro-extraction (SPME), QuEChERS, and Liquid Phase Micro-extraction (LPME).

Published in	International Journal of Pharmacy and Chemistry (Volume 6, Issue 6)
DOI	10.11648/j.ijpc.20200606.11
Page(s)	65-76
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2020. Published by Science Publishing Group

Keywords

Sample Preparation, Pesticide Residues, Food, Extraction, Clean-up

References

[1]	Ji Sun Lee, Soo Hee Cho, Chae Mi Lim, Moon Ik Chang, Hyun Jin Joo, Hojae Bae, Hyun Jin Park. (2017). A Liquid Chromatography - Tandem Mass Spectrometry Approach for the Identification of Mebendazole Residue in Pork, Chicken and Horse. 12 (1). doi: 10.1371/journal.pone.0169597.
[2]	Simone M., Goulart, Renata D. Alves, Washington X. de Paul José Humberto de Queiroz, Antônio A. Nevesa and Maria Eliana L. R. de Queiroz. (2012). Determination of Carbamates in Beverages by Liquid-Liquid Extraction with Low Temperature Partitioning and Liquid Chromatography. J. Braz. Chem. Soc, 23, 1154-1165. doi: 10.1590/S0103-50532012000600022.
[3]	Tesfa Bedassa, Negussie Megersa and Abera Gure. (2017). Salting-out Assisted Liquid-Liquid Extraction for the Determination of Multiresidue Pesticides in Alcoholic Beverages by High Performance Liquid Chromatography. Science Journal of Analytical Chemistry, 5 (3), 38-45. doi: 10.11648/j.sjac.20170503.11.
[4]	Asha LAL, Guanhuat TAN, and Meekin CHAI. (2008). Multiresidue Analysis of Pesticides in Fruits and Vegetables Using Solid-Phase Extraction and Gas Chromatographic Methods. Analytical sciences, 24, 231-236.
[5]	Guo C, Hu JY, Chen XY, Li JZ. (2008). Analysis of Imazaquin in Soybeans by Solid-phase Extraction and High-performance Liquid Chromatography. Bull. Environ. Contam, 80, 173–177.
[6]	Guocan Zheng, Chao Han, Yi Liu, Jing Wang, Meiwen Zhu, Chengjun Wang, and Yan Shen (2014). Multiresidue analysis of 30 organochlorine pesticides in milk and milk powder by gel permeation chromatography-solid phaseextraction-gas chromatography-tandem mass spectrometry. J. Dairy Sci., 97, 6016–6026. Retrieved from dx.doi.org/ 10.3168/jds.2014-8192.
[7]	Hu JY, Zhen ZH, Deng ZB. (2011). Simultaneous Determination of Acetochlor and Propisochlor Residues in Corn and Soil by Solid Phase Extraction and GasChromatography with Electron Capture Detection. Bull. Environ. Contam. Toxicol., 86, 95-100.
[8]	Ravelo-Pérez, J. Hernández-Borges, M. Rodríguez-Delgado. (2008). J. Chromatogr. A, 1211, 33.
[9]	Van der Lee, G. van der Weg, W. A. Traag, G. J. M. Hans. (2008). J. Chromatogr. A, 1186, 325.
[10]	Wu S, Mei J. (2011). Analysis of the Herbicide Bispyribac-sodium in Rice by Solid Phase Extraction and High Performance Liquid Chromatography. Bull. Environ. Contam., 86, 314–318.
[11]	Pérez-Parada, M. C.-A. (2011). J. Chromatogr. A 2011, 1218, 5852.
[12]	Adriana N. Macedo, Ana R. A. Nogueira, Silvia Helena Govoni Brondi. (2009). Matrix Solid-Phase Dispersion Extraction for Analysis of Cypermethrin Residue in Cows’ Milk. chromatographia, 69, 571–573.
[13]	Érica A. Souza-Silvaa, Viorica Lopez-Avilab, Janusz Pawliszyna. (2013). Fast and robust direct immersion solid phase microextraction coupled with gas chromatography–time-of-flight mass spectrometry method employing a matrix compatible fiber for determination of triazolefungicides in fruits. Journal of Chromatography A. Retrieved from www.elsevier.com/locate/chroma.
[14]	Fernandez-Alvarez, M. Llompart, J. P. Lamas, M. Lores, C. Garcia-Jares, R. Cela, T. Dagnac. (2009). J. Chromatogr. A, 1216, 2832.
[15]	Chai, G. H. Tan. (2009). Food Chem, 117, 561.
[16]	Maria Geovania Dantas Silva, Adriano Aquino, Haroldo Silveira D ˆ orea, Sandro Navickiene ´. (2008). Simultaneous determination of eight pesticide residues in coconut using MSPD and GC/MS. Talanta 2008, 76, 680–684. doi: 10.1016/j.talanta.2008.04.018.
[17]	Matrix Solid-Phase Dispersion Extraction for Analysis of Cypermethrin Residue in Cows’ Milk. (2009). Chromatographia, 69, 571–573.
[18]	Sandro Navickiene, Adriano Aquino and Débora Santos Silva Bezerra. (2010). A Matrix Solid-Phase Dispersion Method for theExtraction of Seven Pesticides from Mango and Papaya. chromatographic science. doi: 10.1093/chromsci/48.9.750.
[19]	Tsochatzis ED, Menkissoglu-Spiroudi U, Karpouzas D G, Tzimou-Tsitouridou R. (2010). Anal. Bioanal. Chem., 397, 2181-2190.
[20]	Elham JAHANMARD, Fatemeh ANSARI, Mansour FEIZI. (2016). Evaluation of Quechers Sample Preparation and GC Mass Spec-trometry Method for the Determination of 15 Pesticide Residues in Tomatoes Used in Salad Production Plants. Iran J Public Health, 45, 230-238. Retrieved from http://ijph.tums.ac.ir.
[21]	Chen, P. Y. Cao, R. J. Liu,. (2011). Food Chem, 125, 1406.
[22]	Godfred Darko, Jonah Addai Tabi, Michael Kodwo Adjaloo, and Lawrence Sheringham Borquaye1. (2017). Pesticide Residues in Honey from the Major Honey Producing Forest Belts in Ghana. Journal of Environmental and Public Health. Doi: doi.org/10.1155/2017/7957431.
[23]	Mustapha F. A. Jallow, Dawood G. Awadh, Mohammed S. Albaho, Vimala Y. Devi and Nisar Ahmad. (2017). Monitoring of Pesticide Residues in Commonly Used Fruits and Vegetables in Kuwait. International journal of Enviromental Research and public Health.
[24]	Viñas, N. Campillo, N. Martínez-Castillo, M. Hernández-Córdoba. (2009). J. Chromatogr. A, 1216, 40.
[25]	R. Romero-Gonzáleza,, A. Garrido Frenicha, J. L. Martínez Vidala, O. D. Prestesb, S. L. Grioc. (2011). Simultaneous determination of pesticides, biopesticides and mycotoxins in organic products applying a quick, easy, cheap, effective, rugged and safe extraction procedure and ultra-high performance liquid chromatography–tandem mass spectrometry. Journal of Chromatography A, 1218, 1477–1485. Retrieved from www.elsevier.com/locate/chroma.
[26]	S. C. TRANa, H. TH. LEa and T. H. THAI-NGUYENb. (2015). Determination of pesticide multi-residues in green tea using a modified quechers extraction and liquid chromatography tandem mass spectrometry technique. Acta Alimentaria, 44 (3), 409–419. doi: 10.1556/066.2015.44.0012.
[27]	A. Garbi, V. S. (2010). Talanta, 82, 1286.
[28]	Abera Gure, Francisco J. Lara, Negussie Megersa, Monsalud del Olmo-Iruela & Ana M. García-Campaña. (2014). Dispersive Liquid–Liquid Microextraction Followed by Capillary High-Performance Liquid Chromatography for the Determination of Six Sulfonylurea Herbicides in Fruit Juices. Food Analytical Methods, 7, 1468-1476. doi: 10.1007/s12161-013-9775-5.
[29]	E. Sobhanzadeh, N. K. A. Bakar, M. R. B. Abas, K. Nemati. (2011). J. Hazard. Mater., 186, 1308.
[30]	Elpiniki G. Amvrazi a, Asimina T. Papadi-Psyllou a & Nikolaos G. Tsiropoulos. (2010). Pesticide enrichment factors and matrix effects on the determination of multiclass pesticides in tomato samples by single-drop microextraction (SDME) coupled with gas chromatography andcomparison study between SDME andacetone-partition extraction procedure. International Journal of Environmental Analytical Chemistry, 90, 245-259. doi: 10.1080/03067310903166699.
[31]	Ercheng Zhao, Lijun Han, Shuren Jiang, Qiuxia Wang, Zhiqiang Zhou. (2008). Application of a single-drop microextraction for the analysis of organophosphorus pesticides in juice. Journal of Chromatography A, 1114, 269–273.
[32]	Francisco Barahonaa, Astrid Gjelstadb, Stig Pedersen-Bjergaardb, Knut Einar Rasmussenb. (2010). Hollow fiber-liquid-phase microextraction of fungicides from orange juices. Journal of Chromatography A, 1217, 1989–1994. doi: 10.1016/j.chroma.2010.01.077.
[33]	G. Matsadiq, H. H. (2011). J. Chromatogr. B, 879, 2113.
[34]	J. H. Zhang, H. X. Gao, B. Peng, S. Q. Li, Z. Q. Zhou,. (2011). J. Chromatogr. A, 1218, 6621.
[35]	J. J. Du, H. Y. Yan, D. D. She, B. M. Liu, G. Y. Yang,. (2010). Talanta, 82, 698.
[36]	M. A. Farajzadeh, M. R. A. Mogaddam, H. Ghorbanpour. (2014). Development of a new microextraction method based on elevated temperature dispersive liquid-liquid microextractionfor determination of triazole pesticides residues in honey bygas chromatography-nitrogen phosphorus detection. Journal of chromatographia A. doi: http://dx.doi.org/doi:10.1016/j.chroma.2014.04.067.
[37]	Majid Arvand a, Elahe Bozorgzadeh a, Shahab Shariati. (2013). Two-phase hollow fiber liquid phase microextraction for preconcentration of pyrethroid pesticides residues in some fruits and vegetable juices prior to gas chromatography/mass spectrometry. Journal of Food Composition and Analysis, 31, 275–283. Retrieved from www.els evier.c om/lo cat e/jfca.
[38]	Maosheng Zhang, Jiarong Huangc, Changlin Wei c, Binbin Yu a, Xiaoqing Yang d, Xi Chena. (2007). Mixed liquids for single-drop microextraction of organochlorine pesticides in vegetables. Talanta, 599–604.
[39]	Miguel Ángel González-Curbelo, Javier Hernández-Borges, Teresa María Borges-Miquel, Miguel Ángel Rodríguez-Delgado. (2013). Determination of organophosphorus pesticides and metabolites incereal-based baby foods and wheat flour by means ofultrasound-assisted extraction and hollow-fiber liquid-phasemicroextraction prior to gas chromatography with nitrogenphosphorus detection. Journal of Chromatography A. doi: doi.org/10.1016/j.chroma.2013.05.081.
[40]	Mir Ali Farajzadeh, Mahdi Bamorowat and Mohammad Reza Afshar Mogaddam. (2016). Development of a dispersive liquid–liquid microextraction method based on solidification of a floating ionic liquid for extraction of carbamate pesticides from fruit juice and vegetable samples. RSC Adv, 6, 112939. doi: 10.1039/c6ra20103b.
[41]	S. Pedersen-Bjergaard, K. E. Rasmussen. (2008). J. Chromatogr. A, 1184, 132.
[42]	S. C. Cunha, J. O. Fernandes, M. B. P. P. Oliveira. (2009). J. Chromatogr. A, 1216, 8835.
[43]	Xiaojin Sun, Fang Zhu, Jiabin Xi, Tongbu Lu, Hong Liu, Yexiang Tong, Gangfeng Ouyang. (2011). Hollow fiber liquid-phase microextraction as clean-up step for the determination of organophosphorus pesticides residues in fish tissue by gas chromatographycoupled with mass spectrometry. Marine Pollution Bulletin, 63, 102–107. doi: 10.1016/j.marpolbul.2011.03.038.

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Shibiru Eticha. (2020). A Review: Sample Preparation Methods for the Pesticide Residue Analysis in Food Samples. International Journal of Pharmacy and Chemistry, 6(6), 65-76. https://doi.org/10.11648/j.ijpc.20200606.11

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ACS Style

Shibiru Eticha. A Review: Sample Preparation Methods for the Pesticide Residue Analysis in Food Samples. Int. J. Pharm. Chem. 2020, 6(6), 65-76. doi: 10.11648/j.ijpc.20200606.11

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AMA Style

Shibiru Eticha. A Review: Sample Preparation Methods for the Pesticide Residue Analysis in Food Samples. Int J Pharm Chem. 2020;6(6):65-76. doi: 10.11648/j.ijpc.20200606.11

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@article{10.11648/j.ijpc.20200606.11,
  author = {Shibiru Eticha},
  title = {A Review: Sample Preparation Methods for the Pesticide Residue Analysis in Food Samples},
  journal = {International Journal of Pharmacy and Chemistry},
  volume = {6},
  number = {6},
  pages = {65-76},
  doi = {10.11648/j.ijpc.20200606.11},
  url = {https://doi.org/10.11648/j.ijpc.20200606.11},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ijpc.20200606.11},
  abstract = {The pesticide residues in foods have received increasing attention as one of the most important food safety issues. Therefore, more strict regulations on the maximum residue limits (MRLs) for pesticides in foods have been established in many countries and health organizations, based on the sensitive and reliable analysis methods of pesticide residues. However, the analysis of pesticide residues is a continuing challenge mainly because of the small quantities of analytes as well as the large amounts of interfering substances which can be co-extracted with them, often leading to experimental errors and damage to the Analytical instruments. Thus, extensive sample preparation is often required for the pesticide residue analysis for the effective extraction of the analytes and removal of the interferences. This paper focuses on reviewing the recent development in the sample preparation methods for the pesticide residue analysis in some food samples. The methods include: Liquid-Liquid extraction (LLE), Solid-Phase extraction (SPE), Matrix Solid-Phase Dispersion (MSPD), Solid-Phase Micro-extraction (SPME), QuEChERS, and Liquid Phase Micro-extraction (LPME).},
 year = {2020}
}

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TY  - JOUR
T1  - A Review: Sample Preparation Methods for the Pesticide Residue Analysis in Food Samples
AU  - Shibiru Eticha
Y1  - 2020/11/11
PY  - 2020
N1  - https://doi.org/10.11648/j.ijpc.20200606.11
DO  - 10.11648/j.ijpc.20200606.11
T2  - International Journal of Pharmacy and Chemistry
JF  - International Journal of Pharmacy and Chemistry
JO  - International Journal of Pharmacy and Chemistry
SP  - 65
EP  - 76
PB  - Science Publishing Group
SN  - 2575-5749
UR  - https://doi.org/10.11648/j.ijpc.20200606.11
AB  - The pesticide residues in foods have received increasing attention as one of the most important food safety issues. Therefore, more strict regulations on the maximum residue limits (MRLs) for pesticides in foods have been established in many countries and health organizations, based on the sensitive and reliable analysis methods of pesticide residues. However, the analysis of pesticide residues is a continuing challenge mainly because of the small quantities of analytes as well as the large amounts of interfering substances which can be co-extracted with them, often leading to experimental errors and damage to the Analytical instruments. Thus, extensive sample preparation is often required for the pesticide residue analysis for the effective extraction of the analytes and removal of the interferences. This paper focuses on reviewing the recent development in the sample preparation methods for the pesticide residue analysis in some food samples. The methods include: Liquid-Liquid extraction (LLE), Solid-Phase extraction (SPE), Matrix Solid-Phase Dispersion (MSPD), Solid-Phase Micro-extraction (SPME), QuEChERS, and Liquid Phase Micro-extraction (LPME).
VL  - 6
IS  - 6
ER  -

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Author Information

Shibiru Eticha

Department of Chemistry, Oda Bultum University, Chiro, Ethiopia

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APA Style

Shibiru Eticha. (2020). A Review: Sample Preparation Methods for the Pesticide Residue Analysis in Food Samples. International Journal of Pharmacy and Chemistry, 6(6), 65-76. https://doi.org/10.11648/j.ijpc.20200606.11

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ACS Style

Shibiru Eticha. A Review: Sample Preparation Methods for the Pesticide Residue Analysis in Food Samples. Int. J. Pharm. Chem. 2020, 6(6), 65-76. doi: 10.11648/j.ijpc.20200606.11

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AMA Style

Shibiru Eticha. A Review: Sample Preparation Methods for the Pesticide Residue Analysis in Food Samples. Int J Pharm Chem. 2020;6(6):65-76. doi: 10.11648/j.ijpc.20200606.11

Copy | Download

@article{10.11648/j.ijpc.20200606.11,
  author = {Shibiru Eticha},
  title = {A Review: Sample Preparation Methods for the Pesticide Residue Analysis in Food Samples},
  journal = {International Journal of Pharmacy and Chemistry},
  volume = {6},
  number = {6},
  pages = {65-76},
  doi = {10.11648/j.ijpc.20200606.11},
  url = {https://doi.org/10.11648/j.ijpc.20200606.11},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ijpc.20200606.11},
  abstract = {The pesticide residues in foods have received increasing attention as one of the most important food safety issues. Therefore, more strict regulations on the maximum residue limits (MRLs) for pesticides in foods have been established in many countries and health organizations, based on the sensitive and reliable analysis methods of pesticide residues. However, the analysis of pesticide residues is a continuing challenge mainly because of the small quantities of analytes as well as the large amounts of interfering substances which can be co-extracted with them, often leading to experimental errors and damage to the Analytical instruments. Thus, extensive sample preparation is often required for the pesticide residue analysis for the effective extraction of the analytes and removal of the interferences. This paper focuses on reviewing the recent development in the sample preparation methods for the pesticide residue analysis in some food samples. The methods include: Liquid-Liquid extraction (LLE), Solid-Phase extraction (SPE), Matrix Solid-Phase Dispersion (MSPD), Solid-Phase Micro-extraction (SPME), QuEChERS, and Liquid Phase Micro-extraction (LPME).},
 year = {2020}
}

Copy | Download

TY  - JOUR
T1  - A Review: Sample Preparation Methods for the Pesticide Residue Analysis in Food Samples
AU  - Shibiru Eticha
Y1  - 2020/11/11
PY  - 2020
N1  - https://doi.org/10.11648/j.ijpc.20200606.11
DO  - 10.11648/j.ijpc.20200606.11
T2  - International Journal of Pharmacy and Chemistry
JF  - International Journal of Pharmacy and Chemistry
JO  - International Journal of Pharmacy and Chemistry
SP  - 65
EP  - 76
PB  - Science Publishing Group
SN  - 2575-5749
UR  - https://doi.org/10.11648/j.ijpc.20200606.11
AB  - The pesticide residues in foods have received increasing attention as one of the most important food safety issues. Therefore, more strict regulations on the maximum residue limits (MRLs) for pesticides in foods have been established in many countries and health organizations, based on the sensitive and reliable analysis methods of pesticide residues. However, the analysis of pesticide residues is a continuing challenge mainly because of the small quantities of analytes as well as the large amounts of interfering substances which can be co-extracted with them, often leading to experimental errors and damage to the Analytical instruments. Thus, extensive sample preparation is often required for the pesticide residue analysis for the effective extraction of the analytes and removal of the interferences. This paper focuses on reviewing the recent development in the sample preparation methods for the pesticide residue analysis in some food samples. The methods include: Liquid-Liquid extraction (LLE), Solid-Phase extraction (SPE), Matrix Solid-Phase Dispersion (MSPD), Solid-Phase Micro-extraction (SPME), QuEChERS, and Liquid Phase Micro-extraction (LPME).
VL  - 6
IS  - 6
ER  -

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